华北农学报 ›› 2011, Vol. 26 ›› Issue (S1): 238-240. doi: 10.7668/hbnxb.2011.S1.048

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新型保鲜剂1-甲基环丙烯的顶空气相色谱测定方法研究

陈明, 邵明诚, 魏瑞成, 王冉   

  1. 江苏省食品质量安全重点实验室农业部食用农产品安全监控重点开放实验室江苏省畜禽产品安全性研究重点实验室, 江苏 南京 210014
  • 收稿日期:2010-11-20 出版日期:2011-12-30
  • 作者简介:陈明(1964-),男,上海人,副研究员,主要从事农产品质量安全检测研究。
  • 基金资助:
    中华人民共和国农业部行业标准制定项目(农财发[2008]74号)

Determination of New Fresh-keeping Agent 1-methylcyclopropene by Headspace Gas Chromatography

CHEN Ming, SHAO Ming-cheng, WEI Rui-cheng, WANG Ran   

  1. Key Lab of Food Quality and Safety of Jiangsu Province, Key Open Laboratory of Edible Agricultural Products Safe Monitoring and Control, Ministry of Agriculture, Jiangsu Provincial Key Laboratory of Animal-Derived Food Safety, Nanjing 210014, China
  • Received:2010-11-20 Published:2011-12-30

摘要: 研究建立了新型保鲜剂1-甲基环丙烯的气相色谱顶空气检测方法。采用活性氧化铝填充柱(3 m×3 mm,30~60目)分离,配有氢火焰离子化检测器(FID),异丁烯外标定量。异丁烯和1-甲基环丙烯浓度与检测峰面积值呈良好的线性关系。方法简便、快速、准确。

关键词: 保鲜剂, 1-甲基环丙烯, 异丁烯, 气相色谱顶空法

Abstract: A method has been developed for determination of new fresh-keeping agent 1-methylcyclopropene by headspace gas Chromatography.The samples were separated by a glass packed-column(3 m × 3 mm;30-60 mesh:active alumina),a flame ionization detector(FID) and external standard quantification by isobutylene.The results showed that the peak area response has good linear relationship with isobutylene concentration and 1-methylcyclopropene concentration.The method is simple,rapid and precise.

Key words: Fresh-keeping agent 1-methylcyclopropene, Isobutylene, Headspace gas chromatography

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引用本文

陈明, 邵明诚, 魏瑞成, 王冉. 新型保鲜剂1-甲基环丙烯的顶空气相色谱测定方法研究[J]. 华北农学报, 2011, 26(S1): 238-240. doi: 10.7668/hbnxb.2011.S1.048.

CHEN Ming, SHAO Ming-cheng, WEI Rui-cheng, WANG Ran. Determination of New Fresh-keeping Agent 1-methylcyclopropene by Headspace Gas Chromatography[J]. ACTA AGRICULTURAE BOREALI-SINICA, 2011, 26(S1): 238-240. doi: 10.7668/hbnxb.2011.S1.048.

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